***** Physical Methods of Biochemistry - Fall 2009 *****

Instructor: David W. Hoffman, Associate Professor, Dept of Chemistry & Biochemistry
Office: Room 3.422FA MBB (at the north end of 3.422)
Office hours: Mon & Thurs noon - 1 pm, or by appointment.
Email:  dhoffman@mail.utexas.edu

Class meeting: Tuesday & Thursday 9:30 AM, in Welch 2.256
Class unique number:  54230

Textbook:  Mostly, the course will be based on class notes. If you want to buy a book, a course text "Principles of Physical Biochemistry" by K.E. van Holde, W.C. Johnson & P.S. Ho, 2nd edition (2005) ISBN # 0130464279 is available for those who want.  The textbook is optional, not required.

Schedule for Fall 2009

Thur Aug 27     Course organization; amino acids & proteins.  HW #1 (2 pages, PDF file) 
                              some notes 
Tues Sept 1       Similarity among proteins, multiple sequence alignment and structure.
                               slides from 2nd class  

Thur Sept 3       Nucleic acids - common motifs, stability, hypochromism.   some notes  

Tues Sept 8       Electrophoresis, IEF.  some notes  
Thur Sept 10     Analytical ultracentrifugation, sedimentation.  some notes
Tues Sept 15     Separation of proteins, protein purification.  some notes 
Thur Sept 17     Mass spectrometry.      ** hw # 1 due **   some notes 
Tues Sept 22     Fluorescence.   some notes
Thur Sept 24     Ligand binding.   some notes  
Tues Sept 29     Isothermal titration calorimetry (ITC)  some notes                       
Thur Oct 1        Surface plasmon resonance (SPR)  some notes 
 
Tues Oct 6        *** Midterm exam #1 ***       ** hw # 2 due **

Thur Oct 8        Structure determination; X-ray crystallography  some notes
Tues Oct 13      Structure determination, continued   class notes 
Thur Oct 15      Structure determination, continued  class notes
Tues Oct 20      Structure determination, continued  class notes   
Thur Oct 22      Structure determination, continued  class notes  
Tues Oct 27      last day of x-ray crystallography  class notes  
Thur Oct 29      Small angle x-ray scattering (SAXS)   class notes 
Tues Nov 3       IR and Raman spectroscopy, and CD.  class notes   hw #3    ** hw # 3 due **

Thur Nov 5       Single molecule methods.  class notes 
Tues Nov 10     *** Midterm exam #2 ***      
Thur Nov 12     NMR spectroscopy  class notes  
Tues Nov 17     NMR spectroscopy (continued)  class notes   wuthrich nobel lecture      
Thur Nov 19     NMR spectroscopy (continued)  class notes   
Tues Nov 24     NMR for studying molecular motions
Thur Nov 26     Thanksgiving holiday. 
Tues Dec 1        Cryo-EM    *** hw # 4 due ***   hw #4  
Thur Dec 3        topic to be determined. 

Final exam:  Date and time is set by the university registrar.
According to the registrar's web page, the final is Friday Dec. 11, 9 am - noon.

Grading: Midterm exam #1, midterm exam #2: about 100 pts each; final exam: about 200 pts.
Homeworks, about 50 pts each. 

Course grades will be based on total points earned.  Grades will likely be as follows:

 
   A    93 % of possible points ; A-  90% of possible points
   B+  87% to 90% ; B  83% to 87% ; B-  80 to 83 %
   C+  77% to 80% ; C  73% to 77% ; C-  70 to 73 %
   D+  67% to 70% ; D  63% to 67% ; D-  60 to 63 %
   F   < 60 % of possible points

There will not be make up exams, except under extraordinary circumstances.  There is no excuse for over-sleeping - use two alarms to wake up if necessary.

Homework: There will be four graded homework assignments. Homework will not be accepted late, except under truly extraordinary circumstances, such as a documented medical emergency.  I intend to be strict with this, so plan ahead, and start working on your homework early.

Note regarding homework assignments:  You may discuss your homework with the instructor, TAs, and other students in the class.  But the work that you turn in must be your own.  Do not copy another person's work.

Homework may be typed or handwritten, or some combination of these.  But the homework that you turn in should be neat and well organized.

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